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Volume Resistivity (Pressure probe)
¡Ü Equipment

¨Í Ohm-meter : Equipment having a range of 104 to 10-5 ohms with accuracy of ¡¾02 percent of reading.
¨Î Thickness gauge : Equipped with .750 inch diameter foot anvil and measuring in increments of .001 inch under 4 ounces load.
¨Ï Silver- or gold-plated electrodes : Having a contacting surface area equal to .25 square inch (.564 inch diameter) with suitable provisions for attaching ohm-meter leads.
¨Ð Appropriate fixture or apparatus having capabilities of supporting silver electrodes, test specimen, and suitable means of applying 100 psi pressure across contacting surface area of specimen between electrodes (or 25 pounds force).



NOTES;
1. Dimensions are in inches.
2. Metric equivalents (in parentheses) are given for general information only.


¡Ü Preparation of materials for testing.
The material to be tested shall consist of;
¨Í Test specimens with a thickness of .055 to .120 inch. Use disk of .564¡¾010 inch diameter.
¨Î The surface of the material shall be clean and free of dirty, foreign matter, and indentation.
¨Ï The specimens shall be conditioned for at least three ours at standard temperature of 23¡É¡¾5¡É and at 45 to 75 percent RH in accordance with MIL-STD-202.

¡Ü Preparation of testing electrodes.
¨Í For minimal contact resistance, electrodes shall be cleaned by wiping with alcohol prior to using.
¨Î Electrodes must be properly aligned and contact faces must be flat and parallel to each other.

¡Ü Test procedure.
¨Í Measure and record thickness of material at contact areas to be tested using thickness gauge.
¨Î Material being tested must have sufficient area to contact entire electrode area.
¨Ï Position material between electrodes and apply pressure of 100¡¾5 psi across contact surface area
(25pounds load or force).
¨Ð Maintain constant pressure until electrical requirement is met with a maximum time of two minutes.

es. Calculation. Calculate volume resistivity in ohms-cm using the following formula:

Where:
¥ñ = Volume resistivity (ohm-cm)
R = Observed resistance (ohms)
A = Area of specimen (cm2)
L = Thickness of specimen (cm)

 
Volume Resistivity (Surface probe)
The dc volume resistivity of the material shall be measured in accordance with ASTM D991, except that the probe described herein shall be used in conjunction with a milliohmmeter capable of measuring to a minimum of one milliohm. The sample being measured shall be placed on a nonconductive surface. The probe shall be placed on actual part or a .500 inch wide by 3 inches long by .055 to .120 inch thick test sample in such a manner that the weight of the test probe is uniformly distributed on the part or test sample. The entire width of the part shall be in contact with each electrode. After a 30 second stabilization period, the resistance on the ohmmeter shall be recorded. DC volume resistivity shall be calculated in accordance with ASTM D991 as follows: Where:
¥ñ = DC volume resistivity in ohm-cm.
R = Measured resistance in ohms.
A = Smallest cross section area of part or sample between probe electrodes (cm2).
L = Distance between two electrodes in cm, or 2.54 cm.
The test probe shall be a two-point probe as shown on figure, for parts too small to be measured with this probe, a probe with .5 inch electrode separation may be used, but the value for L in the equation shall be 1.27 cm. For smaller parts, the electrode¡¯s width and spacing should be reduced and the calculation should be on the arc length. Each electrode should touch gasket at one point. In the case of an actual part whose cross section configuration makes it difficult or impossible to measure using this method, the .500 inch wide test sample described above, produced by the same process as the actual part, shall be used.



Inches
mm
NOTES
.005
0.13
1. Dimensions are in inches.
.01
0.2
2. Metric equivalents are given for general information only.
.187
4.75
3. Where applicable the probe will be placed on the flat surface of the item.
.500
12.70
4. Unless otherwise indicated, tolerance is¡¾.010 (0.25 mm).
1.000
25.40
 
 
 
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